Lab
Schedule 
Summer
2011
|
Date |
Experiment |
Reading |
Due |
|
05/17 |
Check-In, Project Overview, Thin Layer Chromatography |
|
|
|
05/19 |
UNIT 1: Synthesis of
Benzyltriphenylphosphonium Bromide Thin Layer Chromatography, IR, NMR, GC-MS |
Mayo, Pike, and Trumper pp125-8; 146-152; 179-212; 237-258;
Carey pp 518-519, 552-7; 519-550; 559-566 |
Unit 1 PreLab |
|
05/24 |
UNIT 1: Workup and Spectroscopy |
Focus on IR Spectroscopy |
Unit 2 PreLab Mayo, Questions: 6-11, 6-13, 6-14, 6-15. Due 10/2 |
|
05/26 |
UNIT 2: Preparation of Stilbene |
|
|
|
05/31 |
UNIT 2: Purification of stilbene: Workup and Spectroscopic Analysis |
Focus on NMR Spectroscopy |
Unit 3 PreLab Mayo, Questions: 7-1 thru 7-5. |
|
06/02 |
UNIT 2: Spectroscopic Analysis continued |
Focus on Mass Spectroscopy |
Unit 4 PreLab |
|
06/07 |
UNIT 3: Preparation of Stilbene Dibromide |
|
Unit 2 PostLab |
|
06/09 |
UNIT 4: Preparation of Diphenylacetylene |
SciFinder |
Unit 5/6 PreLab |
|
06/14 |
UNIT 4: Purification of Diphenylacetylene |
|
Unit 3 PostLab |
|
06/16 |
UNIT 5/6: Preparation of Hexaphenylsilole |
|
Unit 4 PostLab |
|
06/21 |
UNIT 5/6: Purification of Hexaphenylsilole |
SciFinder assignment |
|
|
06/23 |
Check-out* |
|
All formal reports |
* No
laboratory
reports will be accepted after 5:00p.m. on June 28, 2011.